EXPERIENCE OF RESEARCHING THE PROCESS OF DE-FIBRATION OF CELLULOSIC MATERIALS AND ANALYSIS OF EQUIPMENT OPERATION: FROM LABORATORY STAND - TO INDUSTRIAL INSTALLATION
Abstract and keywords
Abstract (English):
The article summarizes the first effort of research in creating and operating experimental and industrial installation for garnetting of cellulose-based materials. The experimental device was created on the basis of a household grain crusher, supplemented with a replaceable pegboard rotor, provided with an adjustable inlet and equipped with a suction pneumatic transport of the unfolded product. The device performs garnetting, mechanical grading, and pneumatic transportation of cellulose materials. The article provides examples of garnetting process studies of various materials, such as wood and cotton celluloses of various commodity forms and brands, waste paper, cellulose laboratory prototypes. Recommendations are formulated on the design parameters and garnetting process methods of pulp lap from sulfite wood cellulose from various manufacturers. Recommended specific capacity is 2.5 kg/(m3∙s). The specific energy intensity of the garnetting process is 75 kJ/kg. The power reserve coefficient of the electric motor is 1.5. The circumferential speed of the rotor’s outer edge is at least 45 m/s. The moisture content of the initial pulp ranges from 5 to 10% (rel.). The size of the sieve cells is 5 mm. The specific productivity of mechanical classification of loosened pulp is 1.5 kg/(m2∙s). The bulk density of the unfolded product is from 30 to 120 kg/m3. The experimental setup can be used for carrying out various experimental studies of the cellulose garnetting processes and development of the necessary experimental samples in the laboratory. The article provides an example of creating an industrial plant with a capacity of 500 kg/h for the production of technical sodium-carboxymethyl cellulose of various brands based on these recommendations, followed by an analysis of the experimental unit operation. The industrial plant is based on a hammer mill and is equipped with a suction pneumatic transport. The industrial plant is used for the cellulose folder garnetting for the needs of industrial cellulose derivatives production.

Keywords:
cellulose, pulp, mechanical crusher, pneumatic transport, mechanical grading, fibrous materials, pretreatment of plant raw materials, experimental research, industrial production, garnetting
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References

1. Makarova I.V., Kunichan V.A., Sevodina K.V., Volkova N.N., Legaev A.I. Optimizaciya tverdofaznogo sposoba polucheniya karboksimetilcellyulozy. Vestnik altayskoy nauki. 2014. № 4 (22). S. 311-314.

2. Niskovskaya M.Yu., Cherneckaya N.V., Ul'yanov B.A., Bragina O.A., Bogdanov V.S. K voprosu o poluchenii karboksimetilovyh efirov cellyulozy suspenzionnym sposobom. Sbornik nauchnyh trudov Angarskogo gosudarstvennogo tehnicheskogo universiteta. 2006. № 1. S. 176-179.

3. Svetlov S.A. Razrabotka oborudovaniya proizvodstva natriy-karboksimetilcellyulozy. Himicheskoe i neftegazovoe mashinostroenie. 2019. T. 55. № 6. S. 3-6.

4. Gorshkova T.A., Mikshina P.V., Gur'yanov O.P., Chelnokova S.B. Formirovanie nadmolekulyarnoy struktury rastitel'noy kletochnoy stenki. Obzor. Biohimiya. 2010. T. 75. № 2. S. 196-213.

5. Lev-Yadun S. Plant fibers: initiation, growth, model plants, and open questions. Fiziologiya rasteniy. 2010. T. 57. № 3. S. 323-333.

6. Loginova S.V., Latuga A.A. Model' struktury izmel'chennoy cellyulozy. Vestnik Moskovskogo gosudarstvennogo universiteta lesa - Lesnoy vestnik. 2016. T. 20. № 2. S. 132-136.

7. Podgorbunskih E.M., Bulina N.V., Bychkov A.L., Lomovskiy O.I. Razuporyadochenie kristallicheskoy struktury cellyulozy pri mehanicheskoy aktivacii. Zhurnal strukturnoy himii. 2018. T. 59. № 1. S. 204-211. URL: https://doi.org/10.1134/S0022476618010328

8. Huang L., Wu Q., Wang Q., Wolcott M. Mechanical activation and characterization of micronized cellulose particles from pulp fiber. Industrial Crops and Products. 2019. V. 141. 111750. URL: https://doi.org/10.1016/j.indcrop.2019.111750

9. Lee H., Mani S. Mechanical pretreatment of cellulose pulp to produce cellulose nanofibrils using a dry grinding method. Industrial Crops and Products. 2017. V. 104. R. 179-187. URL: http://dx.doi.org/10.1016/j.indcrop.2017.04.044

10. Kuhlenko A.A., Orlov S.E., Karpov A.G., Ivanova D.B., Ivanov O.S., Vasilishin M.S., Bereschinova M.N. Issledovanie processa schelochnoy delignifikacii plodovyh obolochek ovsa v rotorno-pul'sacionnom apparate metodami matematicheskogo planirovaniya eksperimenta. Himicheskaya tehnologiya. 2015. T. 16. № 7. S. 443-447.

11. Skiba E.A., Baibakova O.V., Budaeva V.V., Pavlov I.N., Vasilishin M.S., Makarova E.I., Sakovich G.V., Ovchinnikova E.V., Banzaraktsaeva S.P., Vernikovskaya N.V., Chumachenko V.A. Pilot technology of ethanol production from oat hulls for subsequent conversion to ethylene. Chemical Engineering Journal. 2017. V. 329. R. 178–186. DOI:https://doi.org/10.1016/j.cej.2017.05.182

12. Shamin K.I., Chernov A.A., Zotov V.G., Smirnov A.V., Chizhevskiy O.T. Ustroystvo dlya raspushivaniya cellyulozy iz spressovannyh kip: patent RU 149010 U1. Opubl. 20.12.2014.

13. Veselov V.M., Abramov Ya.K., Zalevskiy V.M., Tamurka V.G., Vatueva O.B., Volodin V.S., Gukasov N.A., Marshannikova L.M. Sposob povysheniya kachestva i reakcionnoy sposobnosti cellyulozy: patent RU 2609803 (C1). Opubl. 06.02.2017.

14. Chaschilov D.V. Issledovanie processa razvolokneniya listovoy cellyulozy. Tehnologii i oborudovanie himicheskoy, biotehnologicheskoy i pischevoy promyshlennosti: materialy XIII Vserossiyskoy nauchno-prakticheskoy konferencii studentov, aspirantov i molodyh uchenyh s mezhdunarodnym uchastiem. Biysk: Izd-vo AltGTU, 2020. S. 224-228.

15. Chaschilov D.V. Issledovanie raboty dvuhval'nogo gorizontal'nogo chervyachno-lopastnogo smesitelya v nepreryvnodeystvuyuschem rezhime v proizvodstve natriy-karboksimetilcellyulozy. Tehnologii i oborudovanie himicheskoy, biotehnologicheskoy i pischevoy promyshlennosti: materialy XII Vserossiyskoy nauchno-prakticheskoy konferencii studentov, aspirantov i molodyh uchenyh s mezhdunarodnym uchastiem. Biysk: Izd-vo AltGTU, 2019. S. 349-354.

16. Chaschilov D.V., Kashin A.A. O novom variante metoda ispytaniy cellyulozy na smachivaemost'. Tehnologii i oborudovanie himicheskoy, biotehnologicheskoy i pischevoy promyshlennosti: materialy XI Vserossiyskoy nauchno-prakticheskoy konferencii studentov, aspirantov i molodyh uchenyh s mezhdunarodnym uchastiem. Biysk: Izd-vo AltGTU, 2018. S. 238-243.

17. Vurasko A.V., Minakova A.R., Driker B.N., Spivakov V.P., Kosacheva A.M. Tehnologiya polucheniya cellyulozy iz nedrevesnogo rastitel'nogo syr'ya. Himiya rastitel'nogo syr'ya. 2010. T. 14. № 2. S. 165-168.

18. Yusupov F.T., Saetshin A.A., Valishina Z.T., Borbuzanov V.G., Matuhin E.L. Sovershenstvovanie tehnologiy razvolokneniya, agreagirovaniya i kondicionirovaniya cellyuloznyh materialov. Vestnik tehnologicheskogo universiteta. 2017. T. 20. № 6. S. 76-78.

19. Borbuzanov V.G., Matuhin E.L., Yusupov F.T., Valishina Z.T., Kostochko A.V. Avtomatizirovannyy kompleks podgotovki cellyuloznogo syr'ya novoy fizicheskoy formy. Vestnik Kazanskogo tehnologicheskogo universiteta. 2015. T. 18. № 1. S. 297-299.

20. Antonova N.M., Puzanova A.S., Nebrat A.A. Sravnitel'nyy analiz struktury listovoy i modificirovannoy cellyulozy. Inzhenernyy vestnik Dona. 2020. № 3 (63). S. 39-46.

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